MS Report from Instrument: LCMS-03 File ..018\\20180625\\20180625-1\\CPK2018-625-10209.D Tgt Mass (CHM): Injection Date : 25 Jun 18 3:02 pm +0800 Seq. Line : 56 Sample Name : CPK2018-625-10209 Location : P2-D-11 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\2018\\20180625\\20180625-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\2018\\20180625\\20180625-1\\1-POS-3MIN.M Catalog No : HY-17461A Batch#10209 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off10050000.5 DAD1 B, Sig=254,4 Ref=offmAU1.659100000.5 ELS1 A, ELSD SignalmV50min11.51.79111.51.7181.7181.836mAU22.5min1..885358122.5min00.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7010000005000001.51.74922.500.511.5 Ion 403.5, MSD1 403.5,Target Mass 402.5 +H Positive, EIC=403.2:404.2400000200000000.511.51.74422.5min22.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.72 0.02 182.29 162.65 99.42 403 1.84 0.02 1.06 0.83 0.58 233 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.66 0.01 0.79 0.01 0.26 233 1.72 0.02 294.40 264.68 98.77 403 1.84 0.02 2.49 2.27 0.83 233 1.86 0.01 0.38 0.49 0.13 233 Integration Results for ELS1 A, ELSD Signal RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.79 0.05 299.90 96.20 100.00 403LCMS-03 6/25/2018 3:40:59 PM SYSTEMPage1 of4MS Report from Instrument: LCMS-03 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.75 0.06 5045358.00 1344054.75 100.00 403LCMS-03 6/25/2018 3:40:59 PM SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.75 <<<< POSITIVE SPECTRA >>>> ES-API Positive90000800007000050000404.240000105.120000100000100200300400500600700800900m/z233.130000827.4805.4825.4828.4425.260000403.2LCMS-03 6/25/2018 3:40:59 PM SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 6/25/2018 3:40:59 PM SYSTEMPage4 of4
