Cefprozil_monohydrate_LCMS_16321_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.DSample Name: BIZ2015-513-DJL11-1=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 74Acq. Instrument : HY-LCMS-02 Location : P1-E-04Injection Date : 5/27/2015 6:03:41 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/27/2015 9:09:09 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_6-H01RS10(RP-HPLC.).MLast changed : 5/28/2015 10:58:13 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,MS:100-1000,Column ID:A-RP108 40℃ Catalog No : HY-B0458 Batch#16321 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.D) 1.431 1.326 1.557mAU3503002502001501005000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.326 MM 0.0586 9.72599 2.76694 0.7807 2 1.431 MM 0.0523 1228.19604 391.33014 98.5862 3 1.557 MM 0.0603 7.88720 2.17884 0.6331 Totals : 1245.80923 396.27591 ===================================================================== *** End of Report ***HY-LCMS-02 5/28/2015 11:00:41 AM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.DSample Name: BIZ2015-513-DJL11-1===========================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 74Acq. Instrument : HY-LCMS-02 Location : P1-E-04Injection Date : 5/27/2015 6:03:41 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/27/2015 9:09:09 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_6-H01RS10(RP-HPLC.).MLast changed : 5/28/2015 10:17:06 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,MS:100-1000,Column ID:A-RP108 40℃ Catalog No : HY-B0458 Batch#16321 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.D) ES-API, Pos, S 1.4336000050000400003000020000100000.511.522.53min HY-LCMS-02 5/28/2015 10:17:33 AM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.DSample Name: BIZ2015-513-DJL11-1MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.433 283213 781.20 I 780.20 I 779.20 I 390.10 I 208.05 I 184.00 I*MSD1 SPC, time=1.416:1.471 of D:\\AGLIENT 1260\\DATA\\20150527\\20150527 2015-05-27 09-09-09\\BIZ2015-513-DJL11-1.D ES-A10080Max: 15513 390.16040 184.0 208.1 373.0 391.0200100200300400500600700 *** End of Report ***HY-LCMS-02 5/28/2015 10:17:33 AM Li Shan(LCMS-02)Page

782.2 801.3800m/z 780.2 779.22 of 2